坎地沙坦酯氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.706133061090610706090261997612780.71
213.756266362621626420.05
单位质量响应值RSD%判断
4472.854555.781.30数据可信
氨氯地平--供试品溶液-23020201批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min161527-6152788.37281.828.2488.3781.828.24
249446-4944671.02071.02
358514-5851484.04484.04
461198-6119887.89987.90
553496-5349676.83776.84
657602-5760282.73482.73
10min168021-6802197.69995.434.0597.8595.564.05
261110-6111087.77387.89
366684-6668495.77995.92
466788-6678895.92896.07
568030-6803097.71297.84
668000-6800097.66997.81
15min168178-6817897.92596.742.3598.2397.032.36
264212-6421292.22892.49
367873-6787397.48797.79
468160-6816097.89998.21
568365-6836598.19398.48
667321-6732196.69496.99
20min168699-6869998.67397.671.2699.1598.131.27
266425-6642595.40795.83
367838-6783897.43697.90
468427-6842798.28298.75
568673-6867398.63699.09
667953-6795397.60298.06
30min168491-6849198.37497.810.6799.0198.430.68
267735-6773597.28897.87
367618-6761897.12097.75
468542-6854298.44899.08
568509-6850998.40099.02
667701-6770197.24097.86
45min168438-6843898.29897.800.5199.1098.590.52
267477-6747796.91897.66
368302-6830298.10398.89
467940-6794097.58398.38
568220-6822097.98598.77
668189-6818997.94198.73
60min168260-6826098.04397.021.2899.0197.971.27
266788-6678895.92896.83
367465-6746596.90197.85
466397-6639795.36796.33
568670-6867098.63199.58
667713-6771397.25798.21
极限168133-6813397.86097.100.7198.9998.200.72
266909-6690996.10297.16
367605-6760597.10298.21
467194-6719496.51197.63
568031-6803197.71498.82
667750-6775097.31098.42
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