坎地沙坦酯氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.706133061090610706090261997612780.71
213.756266362621626420.05
单位质量响应值RSD%判断
4472.854555.781.30数据可信
氨氯地平--供试品溶液-23020201批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min161492-6149288.32281.798.2288.3281.798.22
249446-4944671.02071.02
358477-5847783.99183.99
461164-6116487.85087.85
553496-5349676.83776.84
657602-5760282.73482.73
10min167977-6797797.63695.394.0397.7895.524.03
261110-6111087.77387.89
366629-6662995.70095.84
466788-6678895.92896.07
568030-6803097.71297.84
667947-6794797.59397.73
15min168178-6817897.92596.732.3898.2397.022.39
264163-6416392.15892.42
367873-6787397.48797.79
468160-6816097.89998.21
568365-6836598.19398.48
667321-6732196.69496.99
20min168635-6863598.58197.651.2499.0598.101.25
266425-6642595.40795.83
367838-6783897.43697.90
468427-6842798.28298.75
568673-6867398.63699.09
667915-6791597.54798.01
30min168430-6843098.28797.800.6698.9298.420.67
267735-6773597.28897.87
367618-6761897.12097.74
468542-6854298.44899.08
568509-6850998.40099.02
667701-6770197.24097.86
45min168438-6843898.29897.800.5199.1098.580.52
267477-6747796.91897.66
368302-6830298.10398.89
467940-6794097.58398.38
568189-6818997.94198.72
668189-6818997.94198.73
60min168260-6826098.04397.011.3099.0197.961.29
266788-6678895.92896.83
367465-6746596.90197.85
466348-6634895.29696.26
568670-6867098.63199.58
667713-6771397.25798.21
极限168133-6813397.86097.090.7098.9998.190.71
266909-6690996.10297.16
367605-6760597.10298.21
467194-6719496.51197.63
567978-6797897.63898.75
667750-6775097.31098.42
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