替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.872631126252264332648026465263880.39
213.862647126545265080.20
单位质量响应值RSD%判断
1902.521912.550.38数据可信
供试品溶液-js3M批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124220-2422091.46793.892.5691.4793.892.56
224217-2421791.45691.46
324475-2447592.43092.43
425210-2521095.20695.21
525670-2567096.94396.94
625376-2537695.83395.83
10min125491-2549196.26798.702.2897.1899.632.27
225401-2540195.92796.84
326789-26789101.169102.09
426282-2628299.254100.21
526737-26737100.973101.94
626104-2610498.58299.54
15min125566-2556696.55099.722.3298.43101.652.30
226198-2619898.937100.81
326001-2600198.193100.13
427043-27043102.128104.07
526490-26490100.040102.02
627141-27141102.498104.44
20min124545-2454592.69497.392.5395.54100.322.51
225608-2560896.70999.57
326040-2604098.340101.26
426130-2613098.680101.65
526286-2628699.269102.25
626124-2612498.658101.63
30min124289-2428991.72897.122.9095.50101.022.86
225688-2568897.011100.84
325722-2572297.139101.04
426320-2632099.398103.35
526209-2620998.979102.95
626077-2607798.480102.44
45min124433-2443392.27195.982.2496.96100.852.22
225413-2541395.972100.77
325419-2541995.995100.87
425374-2537495.825100.77
525689-2568997.015101.98
626168-2616898.824103.76
60min124745-2474593.45094.801.1899.06100.621.18
225428-2542896.029101.79
324769-2476993.54099.37
425085-2508594.734100.64
525193-2519395.142101.07
625389-2538995.882101.81
极限124443-2444392.30994.101.5998.85100.881.59
224715-2471593.336100.06
324722-2472293.363100.13
425208-2520895.198102.05
524879-2487993.956100.84
625543-2554396.463103.35
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